{"id":90,"date":"2022-04-04T18:44:03","date_gmt":"2022-04-04T16:44:03","guid":{"rendered":"https:\/\/norbertbader.de\/de\/?p=90"},"modified":"2022-04-04T18:44:03","modified_gmt":"2022-04-04T16:44:03","slug":"viscosity-measurement","status":"publish","type":"post","link":"https:\/\/norbertbader.de\/de\/2022\/04\/04\/viscosity-measurement\/","title":{"rendered":"Viscosity measurement"},"content":{"rendered":"\n<h2 class=\"wp-block-heading\">Couette viscometer<\/h2>\n\n\n\n\n\n<p class=\"wp-block-paragraph\">When a liquid is sheared the lubricant exerts a resisting shear stress <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-6eea801fa5ad36923d200f240f3420f9_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#116;&#97;&#117;\" title=\"Rendered by QuickLaTeX.com\" height=\"8\" width=\"10\" style=\"vertical-align: 0px;\"\/> to the motion. The proportion between resistance and certain shear rate <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-055f1f7c1102e5f5dcf1c164a47e82b1_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#100;&#111;&#116;&#123;&#92;&#103;&#97;&#109;&#109;&#97;&#125;&#125;&#61;&#92;&#102;&#114;&#97;&#99;&#123;&#92;&#112;&#97;&#114;&#116;&#105;&#97;&#108;&#32;&#117;&#125;&#123;&#92;&#112;&#97;&#114;&#116;&#105;&#97;&#108;&#32;&#121;&#125;\" title=\"Rendered by QuickLaTeX.com\" height=\"26\" width=\"52\" style=\"vertical-align: -9px;\"\/> may be called viscosity <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-29a7fbaac1a5b0a80f14a4907a848881_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#109;&#117;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"11\" style=\"vertical-align: -4px;\"\/>. By using the definition <\/p>\n\n\n\n<p class=\"wp-block-paragraph\"><a name=\"id3362751475\"><\/a><p class=\"ql-center-displayed-equation\" style=\"line-height: 41px;\"><span class=\"ql-right-eqno\"> (1) <\/span><span class=\"ql-left-eqno\"> &nbsp; <\/span><img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-4fc4e1be31369f2c8f2c54b36538b346_l3.png\" height=\"41\" width=\"80\" class=\"ql-img-displayed-equation quicklatex-auto-format\" alt=\"&#92;&#98;&#101;&#103;&#105;&#110;&#123;&#101;&#113;&#117;&#97;&#116;&#105;&#111;&#110;&#42;&#125;&#92;&#116;&#97;&#117;&#61;&#92;&#109;&#117;&#92;&#99;&#100;&#111;&#116;&#32;&#92;&#102;&#114;&#97;&#99;&#123;&#92;&#112;&#97;&#114;&#116;&#105;&#97;&#108;&#32;&#117;&#125;&#123;&#92;&#112;&#97;&#114;&#116;&#105;&#97;&#108;&#32;&#121;&#125;&#92;&#101;&#110;&#100;&#123;&#101;&#113;&#117;&#97;&#116;&#105;&#111;&#110;&#42;&#125;\" title=\"Rendered by QuickLaTeX.com\"\/><\/p><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">the viscosity can be derived from measurements.  A steady shear experiment with a measurement of the resulting shear force may lead to the possibility to determine the viscosity as shown in Figure 1.<\/p>\n\n\n\n<figure class=\"wp-block-image size-large is-style-default\"><img loading=\"lazy\" decoding=\"async\" width=\"700\" height=\"466\" src=\"https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-700x466.png\" alt=\"\" class=\"wp-image-114\" srcset=\"https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-700x466.png 700w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-300x200.png 300w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-768x511.png 768w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-1536x1022.png 1536w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-2048x1363.png 2048w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscBasic-1568x1043.png 1568w\" sizes=\"auto, (max-width: 700px) 100vw, 700px\" \/><figcaption>Figure 1: Basic Design of a Couette Viscometer<\/figcaption><\/figure>\n\n\n\n<pre class=\"wp-block-preformatted\"><\/pre>\n\n\n\n<p class=\"wp-block-paragraph\">By using a cylinder rotating, at constant speed, in another cylinder a gap filled with liquid of height <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-d8a26bcbb0f1418df30460169d631543_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#104;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"10\" style=\"vertical-align: 0px;\"\/> is sheared. Assuming the linear shear profile the shear rate then is constant across the gap and we can thus simplify <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-bb4004f05344ed6a9725391c31b62982_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#100;&#111;&#116;&#123;&#92;&#103;&#97;&#109;&#109;&#97;&#125;&#32;&#61;&#32;&#92;&#102;&#114;&#97;&#99;&#123;&#117;&#95;&#123;&#92;&#109;&#97;&#116;&#104;&#114;&#109;&#123;&#109;&#97;&#120;&#125;&#125;&#125;&#123;&#104;&#125;\" title=\"Rendered by QuickLaTeX.com\" height=\"19\" width=\"67\" style=\"vertical-align: -6px;\"\/> with dimension of <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-53c006374ed7db7418af8fb08b42f7da_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#102;&#114;&#97;&#99;&#123;&#49;&#125;&#123;&#92;&#109;&#97;&#116;&#104;&#114;&#109;&#123;&#115;&#125;&#125;\" title=\"Rendered by QuickLaTeX.com\" height=\"22\" width=\"7\" style=\"vertical-align: -6px;\"\/>.  The shear stress is given by dividing the measured force <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-6ac8ca8823336a523a19e634714b5d6c_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#70;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"14\" style=\"vertical-align: 0px;\"\/> by the surface area <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-6b6382ec75a998635df10c26959cc8a6_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#116;&#97;&#117;&#32;&#61;&#32;&#92;&#102;&#114;&#97;&#99;&#123;&#70;&#125;&#123;&#65;&#125;\" title=\"Rendered by QuickLaTeX.com\" height=\"22\" width=\"46\" style=\"vertical-align: -6px;\"\/>. It should be noted, that the length must be sufficient to enable a measurement, which is not disturbed by the edge effects. <\/p>\n\n\n\n<p class=\"wp-block-paragraph\">If the speed is too great or the gap to small, the shear stress in the lubricant may reach values leading to different lubricant beahviour. This is mostly a drop in viscosity driven by thermal effects as well non-Newton&#8217;ian effects. These will be adressed in another post.<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">Falling body viscometer<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">Other methods to measure the dynamic viscosity are falling body viscometers as depicted in Fgure 2. <\/p>\n\n\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"700\" height=\"393\" src=\"https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-700x393.png\" alt=\"\" class=\"wp-image-121\" srcset=\"https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-700x393.png 700w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-300x168.png 300w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-768x431.png 768w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-1536x862.png 1536w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-2048x1150.png 2048w, https:\/\/norbertbader.de\/wp-content\/uploads\/2022\/04\/viscFall-1-1568x880.png 1568w\" sizes=\"auto, (max-width: 700px) 100vw, 700px\" \/><figcaption>Figure 2: Falling body viscometer<\/figcaption><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\">By letting a body drop in a tube with known clearance and measureing the velocity that the falling body reaches in the liquid, it is again possible to determine the shear stress. As a direct determination is not readily achievable, these viscometers are usually calibrated using liquids of known viscosity. <\/p>\n\n\n\n<p class=\"wp-block-paragraph\">By varying the gap <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-d8a26bcbb0f1418df30460169d631543_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#104;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"10\" style=\"vertical-align: 0px;\"\/> or the sinker weight (material density) different shear stresses may be reached in the viscometer. The form of the sinker can also influence the stability and repeatability of the falling body setup.<\/p>\n\n\n\n<h2 class=\"wp-block-heading\">Discussion<\/h2>\n\n\n\n<p class=\"wp-block-paragraph\">Using these viscometers usually the viscosity at low shear rates is determined with falling body viscometers. This low shear viscosity <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-b1fc6cbd2a8215f29e267b61a3959cae_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#109;&#117;&#95;&#48;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"18\" style=\"vertical-align: -4px;\"\/> is most commonly used in standard engineering applications. If the shear rate is increased notably using for example Couette viscometers the lubricant viscosity <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-29a7fbaac1a5b0a80f14a4907a848881_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#109;&#117;\" title=\"Rendered by QuickLaTeX.com\" height=\"12\" width=\"11\" style=\"vertical-align: -4px;\"\/> may become shear rate dependent. By forming the ratio of <img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/norbertbader.de\/wp-content\/ql-cache\/quicklatex.com-558af6c3ee6b9f26b3772ac059a2bead_l3.png\" class=\"ql-img-inline-formula quicklatex-auto-format\" alt=\"&#92;&#102;&#114;&#97;&#99;&#123;&#92;&#109;&#117;&#125;&#123;&#92;&#109;&#117;&#95;&#48;&#125;\" title=\"Rendered by QuickLaTeX.com\" height=\"23\" width=\"16\" style=\"vertical-align: -9px;\"\/> it is possible to obtain fluid typical curves, which represent the fluid behaviour. These will be part of the next post.<\/p>\n\n\n\n<div class=\"wp-block-group is-style-default\"><div class=\"wp-block-group__inner-container is-layout-flow wp-block-group-is-layout-flow\">\n<div class=\"wp-block-columns is-style-default is-layout-flex wp-container-core-columns-is-layout-8f761849 wp-block-columns-is-layout-flex\">\n<div class=\"wp-block-column is-layout-flow wp-block-column-is-layout-flow\" style=\"flex-basis:100%\"><\/div>\n<\/div>\n<\/div><\/div>\n\n\n\n<p class=\"wp-block-paragraph\"><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Couette viscometer When a liquid is sheared the lubricant exerts a resisting shear stress $\\tau$ to the motion. The proportion between resistance and certain shear rate $\\dot{\\gamma}}=\\frac{\\partial u}{\\partial y}$ may be called viscosity $\\mu$. By using the definition \\begin{equation}\\label{eq:mu}\\tau=\\mu\\cdot \\frac{\\partial u}{\\partial y}\\end{equation} the viscosity can be derived from measurements. A steady shear experiment with a&hellip; <a class=\"more-link\" href=\"https:\/\/norbertbader.de\/de\/2022\/04\/04\/viscosity-measurement\/\">Continue reading <span class=\"screen-reader-text\">Viscosity measurement<\/span><\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[1],"tags":[5,4],"class_list":["post-90","post","type-post","status-publish","format-standard","hentry","category-general","tag-experiment","tag-viscosity","entry"],"_links":{"self":[{"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/posts\/90","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/comments?post=90"}],"version-history":[{"count":33,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/posts\/90\/revisions"}],"predecessor-version":[{"id":126,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/posts\/90\/revisions\/126"}],"wp:attachment":[{"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/media?parent=90"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/categories?post=90"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/norbertbader.de\/de\/wp-json\/wp\/v2\/tags?post=90"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}